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• W2203094161 abstract "The effect of synthesis techniques on structural, magnetocaloric and critical behavior in Pr0.6Ca0.1Sr0.3Mn0.975Fe0.025O3 (PCSMFO) sample has been investigated. The sample was synthesized by two different methods: the solid-state reaction (SS) and Pechini sol–gel method (SG). X-ray diffraction analysis shows that our sample crystallizes in the orthorhombic structure with the Pbnm space group for both methods. Magnetic measurements show that our sample exhibits a ferromagnetic (FM)–paramagnetic (PM) transition with increasing temperature. The Curie temperature (TC) and magnetocaloric effect (MCE) of SS sample and SG sample were studied. A large magnetocaloric effect around Curie temperature is observed in our sample prepared by both methods. Moreover, the critical exponents β, γ, and δ determined as using the modified Arrott-plot (MAP), the Kouvel–Fisher method (KF), as well as the critical isotherm (CI) analysis. In both studied techniques, the Arrott plots show that the phase transition is of the second-order. Moreover, for the sample which is prepared by solid-state, the estimated critical exponents are close to those expected for mean-field model. For the SG sample, these exponents are close to those expected for 3D-dimensional Heisenberg and the value of critical exponents γ decreased and approached the 3D-Ising (γ=1.24). Interestingly, the change of the universality class can be explained by the reduction of grain size (D). The reduction of the grain size tends to create a transition phase from a long-range to short-range order in the system. These results suggest that the physical properties of our sample are strongly depended on the synthesis techniques." @default.
• W2203094161 created "2016-06-24" @default.
• W2203094161 creator A5011888189 @default.
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• W2203094161 date "2015-11-01" @default.
• W2203094161 modified "2023-10-16" @default.
• W2203094161 title "Effect of synthesis techniques on structural, magnetocaloric and critical behavior of Pr0.6Ca0.1Sr0.3Mn0.975Fe0.025O3 manganites" @default.
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• W2203094161 doi "https://doi.org/10.1016/j.ceramint.2015.06.078" @default.
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