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- W2203810597 abstract "Acid-base bifunctional superparamagnetic FeZrOx nanoparticles were synthesized via a two-step process of solvothermal treatment and hydrolysis-condensation, and were further employed to catalyze the conversion of ethyl levulinate (EL) to gamma-valerolactone (GVL) using ethanol as both H-donor and solvent. ZrFeO(1:3)-300 nanoparticles (12.7 nm) with Fe3O4 core covered by ZrO2 layer (0.65 nm thickness) having well-distributed acid-base sites (0.39 vs 0.28 mmol/g), moderate surface area (181 m(2)/g), pore size (9.8 nm), and strong magnetism (35.4 Am-2 kg(-1)) exhibited superior catalytic performance, giving a high GVL yield of 87.2% at 230 degrees C in 3 h. The combination of the nanoparticles with solid acid HY2.6 promoted the direct transformation of sugars to produce GVL in moderate yield (around 45%). Moreover, the nanocatalyst was easily recovered by a magnet for six cycles with an average GVL yield of 83.9% from EL." @default.
- W2203810597 created "2016-06-24" @default.
- W2203810597 creator A5026127442 @default.
- W2203810597 creator A5054626588 @default.
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- W2203810597 date "2015-12-17" @default.
- W2203810597 modified "2023-09-24" @default.
- W2203810597 title "Direct Conversion of Sugars and Ethyl Levulinate into γ-Valerolactone with Superparamagnetic Acid–Base Bifunctional ZrFeO<sub><i>x</i></sub> Nanocatalysts" @default.
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- W2203810597 doi "https://doi.org/10.1021/acssuschemeng.5b01480" @default.
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