Matches in SemOpenAlex for { <https://semopenalex.org/work/W2211893034> ?p ?o ?g. }
Showing items 1 to 89 of
89
with 100 items per page.
- W2211893034 endingPage "54" @default.
- W2211893034 startingPage "47" @default.
- W2211893034 abstract "In the present work, a viable protocol was developed to prepare monodisperse cellooligomers up to a degree of polymerisation (DP) of 20. Peracetylated cellooligosaccharides were obtained from cellulose by acetolysis and subsequently purified by Normal Phase-High Performance Liquid Chromatography using toluene, ethyl acetate and acetone as eluents. In addition, we demonstrated how to efficiently monitor the purity and dispersity of the obtained compounds by High Performance Thin Layer Chromatography, Matrix-Assisted Laser Desorption/Ionization-Time of Flight Mass Spectrometry and Nuclear Magnetic Resonance. With this approach, it is possible to isolate cellooligomer standards up to DP 20 on a preparative scale (dozens of mg). The column chromatographic separation proved to be robust over several months and to be scalable from a analytical to a preparative column. The isolated oligomer standards allow a more precise description of cellooligomer distributions typically emerging from biorefinery process streams after hydrolysis of lignocelluloses. They can be used to calibrate the oligomeric region in size-exclusion chromatography where light scattering detection fails due to limited scattering intensities." @default.
- W2211893034 created "2016-06-24" @default.
- W2211893034 creator A5002514645 @default.
- W2211893034 creator A5007156360 @default.
- W2211893034 creator A5011495446 @default.
- W2211893034 creator A5030223095 @default.
- W2211893034 creator A5039401033 @default.
- W2211893034 creator A5053619689 @default.
- W2211893034 creator A5072917881 @default.
- W2211893034 date "2016-01-01" @default.
- W2211893034 modified "2023-09-23" @default.
- W2211893034 title "Preparation and analytical characterisation of pure fractions of cellooligosaccharides" @default.
- W2211893034 cites W1524530575 @default.
- W2211893034 cites W1982221625 @default.
- W2211893034 cites W1989081503 @default.
- W2211893034 cites W2004163341 @default.
- W2211893034 cites W2012488641 @default.
- W2211893034 cites W2013949806 @default.
- W2211893034 cites W2019983674 @default.
- W2211893034 cites W2031857143 @default.
- W2211893034 cites W2040392233 @default.
- W2211893034 cites W2043592218 @default.
- W2211893034 cites W2045458502 @default.
- W2211893034 cites W2053623655 @default.
- W2211893034 cites W2054682601 @default.
- W2211893034 cites W2064756756 @default.
- W2211893034 cites W2074449922 @default.
- W2211893034 cites W2074777302 @default.
- W2211893034 cites W2080817335 @default.
- W2211893034 cites W2117688821 @default.
- W2211893034 cites W2157646567 @default.
- W2211893034 cites W2332239282 @default.
- W2211893034 doi "https://doi.org/10.1016/j.chroma.2015.12.090" @default.
- W2211893034 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/26792451" @default.
- W2211893034 hasPublicationYear "2016" @default.
- W2211893034 type Work @default.
- W2211893034 sameAs 2211893034 @default.
- W2211893034 citedByCount "17" @default.
- W2211893034 countsByYear W22118930342016 @default.
- W2211893034 countsByYear W22118930342017 @default.
- W2211893034 countsByYear W22118930342018 @default.
- W2211893034 countsByYear W22118930342019 @default.
- W2211893034 countsByYear W22118930342020 @default.
- W2211893034 countsByYear W22118930342021 @default.
- W2211893034 countsByYear W22118930342022 @default.
- W2211893034 countsByYear W22118930342023 @default.
- W2211893034 crossrefType "journal-article" @default.
- W2211893034 hasAuthorship W2211893034A5002514645 @default.
- W2211893034 hasAuthorship W2211893034A5007156360 @default.
- W2211893034 hasAuthorship W2211893034A5011495446 @default.
- W2211893034 hasAuthorship W2211893034A5030223095 @default.
- W2211893034 hasAuthorship W2211893034A5039401033 @default.
- W2211893034 hasAuthorship W2211893034A5053619689 @default.
- W2211893034 hasAuthorship W2211893034A5072917881 @default.
- W2211893034 hasConcept C11432220 @default.
- W2211893034 hasConcept C162356407 @default.
- W2211893034 hasConcept C178790620 @default.
- W2211893034 hasConcept C181199279 @default.
- W2211893034 hasConcept C185592680 @default.
- W2211893034 hasConcept C193363816 @default.
- W2211893034 hasConcept C43617362 @default.
- W2211893034 hasConceptScore W2211893034C11432220 @default.
- W2211893034 hasConceptScore W2211893034C162356407 @default.
- W2211893034 hasConceptScore W2211893034C178790620 @default.
- W2211893034 hasConceptScore W2211893034C181199279 @default.
- W2211893034 hasConceptScore W2211893034C185592680 @default.
- W2211893034 hasConceptScore W2211893034C193363816 @default.
- W2211893034 hasConceptScore W2211893034C43617362 @default.
- W2211893034 hasLocation W22118930341 @default.
- W2211893034 hasLocation W22118930342 @default.
- W2211893034 hasOpenAccess W2211893034 @default.
- W2211893034 hasPrimaryLocation W22118930341 @default.
- W2211893034 hasRelatedWork W1839441791 @default.
- W2211893034 hasRelatedWork W2016529404 @default.
- W2211893034 hasRelatedWork W2018069544 @default.
- W2211893034 hasRelatedWork W2019498801 @default.
- W2211893034 hasRelatedWork W2043901743 @default.
- W2211893034 hasRelatedWork W2074263550 @default.
- W2211893034 hasRelatedWork W2087207741 @default.
- W2211893034 hasRelatedWork W2093423158 @default.
- W2211893034 hasRelatedWork W2561847501 @default.
- W2211893034 hasRelatedWork W2724449984 @default.
- W2211893034 hasVolume "1431" @default.
- W2211893034 isParatext "false" @default.
- W2211893034 isRetracted "false" @default.
- W2211893034 magId "2211893034" @default.
- W2211893034 workType "article" @default.