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- W2224014964 abstract "Introduction The actinide cation, whatever the oxidation states, is large compared with d-transition element cation and are therefore appreciably more basic in character. Since, the actinide cations decrease in size with increasing atom number – the actinide contraction – the electronic attraction Abstract The reaction of uranyl(VI) sulfate with 15 semicarbazones derived from 4-amino antipyrine in the presence of tetramethylene sulfoxide (TMSO) resulted the complexes of the general composition [UO2SO4(L)•TMSO], where L = 4[N-(benzalidene) amino]antipyrine semicarbazone (BAAPS); 4[N-(2’-hydroxybenzalidene)amino] antipyrine semicarbazone (HBAAPS); 4[N-(4’-methoxybenzalidene)amino]antipyrine semicarbazone (MBAAPS); 4[N-(2’-nitrobenzalidene)amino]antipyrine semicarbazone (2’-NO2BAAPS); 4[N-(3’-nitrobenzalidene)amino]antipyrine semicarbazone (3’NO2BAAPS); 4[N-(4’-nitrobenzalidene)amino]antipyrine semicarbazone (4’NO2BAAPS); 4[N-(4’-dimethylaminobenzalidene)amino]antipyrine semicarbazone (DABAAPS); 4[N-(4’-hydroxy-3’-methoxybenzalidene)amino]antipyrine semicarbazone (HMBAAPS); 4[N-(2’-hydroxy-1’-naphthalidene)amino]antipyrine semicarbazone (HNAAPS); 4[N-(cinnamalidene)amino]antipyrine semicarbazone (CAAPS); 4[N(3’,4’,5’-trimethoxybenzalidene)amino]antipyrine semicarbazone (TMBAAPS); 4[N(furfural)amino]antipyrine semicarbazone (FFAAPS); 4[N-(4’-ethylbenzalidene)amino] antipyrine semicarbazone (EBAAPS); 4[N-(2’,4’-dimethylbenzalidene)amino]antipyrine semicarbazone (DMBAAPS); 4[N-(2’,4’-Dichlorobenzalidene)amino]antipyrine semicarbazone (DCBAAPS). All these complexes were characterized by means of elemental analysis, conductivity measurements, molecular weight, magnetic moments and infrared studies. The coordination number 8 is proposed for the complexes. Thermal properties of the representative complexes are also reported." @default.
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- W2224014964 date "2010-01-01" @default.
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- W2224014964 title "SYNTHESIS, SPECTRAL AND THERMAL PROPERTIES OF MIXED LIGAND COMPLEXES OF URANYL (VI) SULFATE" @default.
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