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- W222808083 abstract "The structure of thin films of refractory metals (W, Mo), deposited from the gas phase by pyrolysis of the corresponding carbonyl vapors at 300--400/sup 0/ C, was studied by x-ray structure and electron-diffraction methods of analysis. It was shown that low-temperature pyrolysis produces a metastable fcc phase, i.e., an interstitial solid solution of variable composition (berthollide phase). Structural transformations in the films during subsequent heat treatment were investigated experimentally. On annealing at 600--800/sup 0/ C, the fcc phase decomposes to form, in the case of W, a bcc lattice with the period....., characteristic of the pure metal, and in that of Mo, the hexagonal molybdenum carbide Mo/sub 2/C. The difference in behavior of Mo and W films on heat treatment is due to the different carbon contents in the initial films (4.2--4.7 wt.% for Mo and 0.7--0.9 wt.% for W according to data of vacuum-chromatographic analysis)." @default.
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- W222808083 date "1977-09-01" @default.
- W222808083 modified "2023-09-27" @default.
- W222808083 title "Structure of tungsten and molybdenum films deposited from the gas phase in the low-temperature pyrolysis of carbonyls" @default.
- W222808083 hasPublicationYear "1977" @default.
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