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• W2237463071 endingPage "1064" @default.
• W2237463071 startingPage "1058" @default.
• W2237463071 abstract "Atmospheric-pressure laser ionization mass spectrometry (APLI-MS) is a powerful method for the analysis of polycyclic aromatic hydrocarbon (PAH) molecules, which are ionized in a selective and highly sensitive way via resonance-enhanced multiphoton ionization. APLI was presented in 2005 and has been hyphenated successfully to chromatographic separation techniques like high performance liquid chromatography (HPLC) and gas chromatography (GC). In order to expand the portfolio of chromatographic couplings to APLI, a new hyphenation setup of APLI and supercritical-fluid chromatography (SFC) was constructed and aim of this work. Here, we demonstrate the first hyphenation of SFC and APLI in a simple designed way with respect to different optimization steps to ensure a sensitive analysis. The new setup permits qualitative and quantitative determination of native and also more polar PAH molecules. As a result of the altered ambient characteristics within the source enclosure, the quantification of 1-hydroxypyrene (1-HP) in human urine is possible without prior derivatization. The limit of detection for 1-HP by SFC-APLI-TOF(MS) was found to be 0.5 μg L–1, which is lower than the 1-HP concentrations found in exposed persons." @default.
• W2237463071 created "2016-06-24" @default.
• W2237463071 creator A5046689115 @default.
• W2237463071 creator A5055073532 @default.
• W2237463071 date "2015-12-15" @default.
• W2237463071 modified "2023-09-29" @default.
• W2237463071 title "SFC-APLI-(TOF)MS: Hyphenation of Supercritical Fluid Chromatography to Atmospheric Pressure Laser Ionization Mass Spectrometry" @default.
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• W2237463071 doi "https://doi.org/10.1021/acs.analchem.5b04402" @default.
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