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• W2239985971 abstract "In this paper, the TiO2@[email protected]2 rattle type core shell structure nanoparticles were prepared through calcination of the precursor [email protected]2 which was synthesized from titanyl oxalate complex (TOC) and tetraethyl orthosilicate (TEOS) with co-precipitation in a mixture solvent of ethanol and ammonia. The TOC was prepared from H4TiO4 and oxalic acid dihydrate, and the mole ratio of H4TiO4 to oxalic acid dihydrate was a key factor to form core shell structure. When the mole ratio was 1–2, the core shell structure nanoparticles with void could be obtained. But if the ratio was 1, we get merely the nanoparticles with uniform mixtures of SiO2 and TiO2. Scanning and transmission electron microscopic techniques (SEM & TEM), particle size distribution, Brunauer–Emmett–Teller method (BET), Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA) and X-ray diffraction method (XRD) were employed to characterize the structure and properties of the final particles as well as the precursors. The diameter of core part, the thickness of void space and the thickness of the shell for the TiO2@[email protected]2 particle were about 60 nm, 2 nm and 12 nm, respectively. The TiO2 core was anatase form. The SiO2 shell was amorphous with ca. 3.5 nm mesopores. Methylene blue (MB) was used to evaluate the photocatalytic property of the TiO2@[email protected]2 particles. The result showed that photodegradation of MB on TiO2@[email protected]O2 gave almost the same degeration ratio as on P-25 at last, but the rattle type structure started its photocatalytic property somewhat slower than P-25." @default.
• W2239985971 created "2016-06-24" @default.
• W2239985971 creator A5015733934 @default.
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• W2239985971 date "2015-11-01" @default.
• W2239985971 modified "2023-09-23" @default.
• W2239985971 title "A new approach to preparation of TiO2@void@SiO2 rattle type core shell structure nanoparticles via titanyl oxalate complex" @default.
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• W2239985971 doi "https://doi.org/10.1016/j.colsurfa.2015.08.036" @default.
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