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W2240696543 abstract "Synthesis and characterization of microsheets, microrods, microflowers and microspheres of orthorhombic phase molybdenum oxide (MoO 3 ) were reported. The reaction between ammonium molybdate and hydrochloric acid was used to prepare MoO 3 microstructures and followed by annealing in air at 400 oC for 2h. The combined techniques of X-ray powder diffraction (XRD), field emission scanning electron microscope (FESEM), transmission electron microscopy (TEM) and Raman spectroscopy were used to investigate the effect of pH and additives on the as-prepared samples. Results indicated that they were of microsize. With alcohol as an additive, the sample was plate-like MoO 3 at pH=2.5, and it was a mixture of MoO 3 and MoO 3 •0.55H 2 O of irradiative corolla at pH=1. The sample obtained by hydrothermal was MoO 3 flowers. Meanwhile, when silane coupling agent was introduced as the additive, the sample was MoO 3 spheres." @default.
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W2240696543 date "2012-07-01" @default.
W2240696543 modified "2023-09-27" @default.
W2240696543 title "Synthesis of MoO<sub>3</sub> Nanostructures by a Solution Method" @default.
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W2240696543 doi "https://doi.org/10.4028/www.scientific.net/amr.554-556.494" @default.
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