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• W2242014879 abstract "Hybrid nanoparticles were prepared by direct polymerization of methyl methacrylate, vinyl acetate, and styrene monomers onto the unmodified hydrophilic surfaces of 33 nm silica nanoparticles in a semi-continuous soap-free emulsion polymerization at a monomer starved condition. The polymerization was initiated by potassium persulfate with constant monomer feed at 0.01, 0.02, or 0.04 mL/min. The growth of the core-shell nanoparticles were measured by a laser particle size analyzer. FT-IR spectra analysis confirmed the hybrid structures of the synthesized nanoparticles. SEM images and size exclusion chromatography (SEC) results indicated regular core-shell microsphere structures. The hybrid nanoparticles increased in monodispersity and size over 100 nm with the reaction. However, SiO 2 /polystyrene (PS) nanoparticles grew much faster compared with SiO 2 /polymethyl methacrylate (PMMA) and SiO 2 /polyvinyl acetate (PVAC). There was particle coagulation, about 12 SiO 2 /PS particles aggregating to one, in the early stage of the seeded process. In addition, PS secondary particles were formed before the particle coagulation, and then merged with the SiO 2 /PS nanoparticles in the particle coagulation. The formation of SiO 2 /polymer hybrid nanoparticles depended on the hydrophilic characteristics of the polymer, and the size of silica seeds." @default.
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• W2242014879 date "2015-07-01" @default.
• W2242014879 modified "2023-09-27" @default.
• W2242014879 title "Preparation of Silica/Polymer Hybrid Nanoparticles via a Semi-Continuous Soup-Free Emulsion Polymerization" @default.
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• W2242014879 doi "https://doi.org/10.4028/www.scientific.net/amr.1120-1121.233" @default.
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