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- W2250874490 abstract "Abstract Interactions between butadiene rubber (BR) and polysulfide silane (TESPT) were studied by liquid state NMR spectroscopy. 1 H, 13 C and DOSY spectra highlighted the presence of pre-crosslinking and grafting reactions in BR/TESPT blends mixed with dump temperatures between 155 and 180 °C. Pre-crosslinking induced by the sulfur release of TESPT was evidenced at high temperature. The grafting rate of silane on BR chains was quantified thanks to deconvolution of 1 H NMR signals of crude blends and 1 H spectra analysis of blends after extraction of non-grafted silane. These two methods showed similar values of grafting rates and demonstrated the influence of the dump temperature on BR/silane reactions." @default.
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- W2250874490 date "2016-03-01" @default.
- W2250874490 modified "2023-10-18" @default.
- W2250874490 title "Rubber/silane reactions and grafting rates investigated by liquid-state NMR spectroscopy" @default.
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- W2250874490 doi "https://doi.org/10.1016/j.polymer.2016.01.055" @default.
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