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- W2254881978 abstract "Abstract An environmentally friendly oxidative cleavage of tetrahydrofuran‐2‐methanols to the corresponding γ‐lactones using a catalytic amount of 2‐iodo‐ N ‐isopropylbenzamide has been developed. The reaction of various tetrahydrofuran‐2‐methanols with the catalyst in the presence of Oxone ® (2 KHSO 5 ⋅KHSO 4 ⋅K 2 SO 4 ) as a co‐oxidant in DMF at room temperature successfully affords the corresponding lactones in good to high yields, and recovery of the catalyst is readily accomplished using a reductive work‐up. This method is notable because it enables the transformation of tetrahydrofuran‐2‐methanols to γ‐lactones under mild conditions without the use of any toxic heavy metals. magnified image" @default.
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- W2254881978 date "2016-02-11" @default.
- W2254881978 modified "2023-10-18" @default.
- W2254881978 title "Efficient Oxidative Cleavage of Tetrahydrofuran-2-methanols to γ-Lactones by a 2-Iodobenzamide Catalyst in Combination with Oxone<sup>®</sup>" @default.
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- W2254881978 doi "https://doi.org/10.1002/adsc.201500795" @default.
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