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- W2276903335 abstract "A variety of ethylarenes were converted into the corresponding primary aromatic amides in good yields via treatment with N-bromosuccinimide in the presence of a catalytic amount of 2,2′-azobis(isobutyronitrile) in a mixture of ethyl acetate and water, acetonitrile and water, or chloroform and water, followed by reaction with molecular iodine and aq NH3 in one pot. It was found that aryl α-bromomethyl ketones and/or aryl methyl ketones were formed at the first reaction step and their iodoform-type reaction occurred at the second reaction step to provide primary aromatic amides. The present reaction is a useful and practical transition-metal-free method for the preparation of primary aromatic amides from ethylarenes." @default.
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- W2276903335 date "2016-01-27" @default.
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- W2276903335 title "Direct Transformation of Ethylarenes into Primary Aromatic Amides with <i>N</i>-Bromosuccinimide and I<sub>2</sub>–Aqueous NH<sub>3</sub>" @default.
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- W2276903335 doi "https://doi.org/10.1021/acs.orglett.6b00048" @default.
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