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• W2278714933 abstract "A solvent-free semihydrogenation of 2-methyl-3-butyn-2-ol (MBY) to 2-methyl-3-buten-2-ol was performed in a capillary reactor (10 m long, 0.53 mm i.d.) coated with a titania supported Pd–Bi catalyst. Several coatings with different Pd/Bi ratio have been prepared. The catalysts have been characterized with SEM, TEM, EDX, XRD analysis and N2 adsorption–desorption measurements. The maximum alkene yield of 90% was obtained at a molar Pd/Bi ratio of 11. The yield was increased to 95% in the presence of 10 mol.% pyridine in the reaction mixture. The alkene selectivity decreased with time due to leaching of Bi. The leaching was fully suppressed in the presence of 1 vol.% acetic acid in the reaction mixture. The catalyst remained stable for 100 h of continuous operation. The results demonstrate that capillary reactors provide alkene selectivity the same compared to ideal stirred tank batch reactors." @default.
• W2278714933 created "2016-06-24" @default.
• W2278714933 creator A5018946182 @default.
• W2278714933 creator A5036620679 @default.
• W2278714933 creator A5081627735 @default.
• W2278714933 date "2016-04-01" @default.
• W2278714933 modified "2023-09-27" @default.
• W2278714933 title "Solvent-free semihydrogenation of acetylene alcohols in a capillary reactor coated with a Pd–Bi/TiO 2 catalyst" @default.
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• W2278714933 doi "https://doi.org/10.1016/j.apcata.2016.01.019" @default.
• W2278714933 hasPublicationYear "2016" @default.
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