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• W2280400566 abstract "A series of vanadium(III) diiodide complexes of the formula CpV(PRNR′PR)I2 [Cp = η5-C5H5; PRNR′PR = (R2PCH2)2N(R′); R = Et, R′ = Me (1a); R = Et, R′ = Ph (1b); R = Ph, R′ = Me (1c)] is reported. The corresponding vanadium(II) monoiodide complexes of the formula CpV(PRNR′PR)I [R = Et, R′ = Me (2a); R = Et, R′ = Ph (2b); R = Ph, R′ = Me (2c)] were prepared in THF by reduction of 1a–c with Zn powder. We report the preparation of the vanadium(II) complexes CpV(PPh2NPh2)I (3) (PPh2NPh2 = 1,3,5,7-tetraphenyl-1,5-diaza-3,7-diphosphacyclooctane) as well as trans-[VCl2(PEtNMePEt)2] (4a) and trans-[VCl2(PEtNPhPEt)2] (4b). These paramagnetic complexes are characterized by elemental analysis, 1H NMR spectroscopy, and cyclic voltammetry for 2a, 2b, 3 and 4b. Complexes 1c, 2a–c, 3, and 4b were also characterized by single-crystal X-ray crystallography. These complexes represent initial examples for the coordination chemistry of vanadium with PRNR′PR and PPh2NPh2 diphosphine ligands, which contain a pendant amino groups in the second coordination sphere." @default.
• W2280400566 created "2016-06-24" @default.
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• W2280400566 date "2016-02-18" @default.
• W2280400566 modified "2023-09-26" @default.
• W2280400566 title "Synthesis and Structure of Vanadium Halide Complexes Containing Diphosphine Ligands with Pendant Amines" @default.
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• W2280400566 doi "https://doi.org/10.1002/ejic.201501477" @default.
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