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- W228130126 abstract "The overall hexa-gonal framework of the title compound, penta-sodium ammonium trimanganese(II) borophosphate sesquihydrate, consists of tube-like borophosphate anions, (∞) (1){[B(3)P(2)O(11)(OH)](4-)}, made up of corner-sharing PO(4) and BO(4) tetra-hedra and BO(2)(OH) triangles, forming ten-membered ring windows. The tubes are inter-connected via distorted MnO(6) octa-hedra, establishing a three-dimensional open-framework structure with two different types of ring-channels (12- and six-membered) that run along [001]. The 12-membered ring channels are occupied by NH(4) (+) ions and water mol-ecules. The ten-membered ring windows in the walls of the tubes are occupied by Na(+) ions. The remaining Na(+) ions and the water mol-ecules, one of which is half-occupied, reside within the six-membered ring channels. The structural setup is consolidated by an O-H⋯O hydrogen bond between the OH group and an opposite O atom of the framework. Donor-acceptor distances ranging from 2.80 to 3.35 Å between the ammonium N atom, water O atoms and framework O atoms indicate further hydrogen-bonding inter-actions." @default.
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- W228130126 date "2008-11-22" @default.
- W228130126 modified "2023-09-27" @default.
- W228130126 title "Na<sub>5</sub>(NH<sub>4</sub>)Mn<sub>3</sub>[B<sub>9</sub>P<sub>6</sub>O<sub>33</sub>(OH)<sub>3</sub>]·1.5H<sub>2</sub>O" @default.
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- W228130126 doi "https://doi.org/10.1107/s1600536808037884" @default.
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