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- W2281881434 abstract "Objective. There have been many studies of the concentrations of elements in blood and urine, but few studies have focused on the concentrations of elements in bone. The elements in bone play, important roles in a variety of physiological processes. The objective of this study was to assess the optimum conditions for measuring the concentrations of 14 elements in human bone samples.Methods. Seventy-seven bone samples were collected from bone surgery patients and pretreated using a microwave digest. Inductively couple plasma-atomic emission spectroscopy (ICP-AES) analysis was used to determine the optimal conditions for three variables: sample uptake rate, flow rate of Argon gas (Ar) into the nebulizer and concentrations of nitric acid.Results. The detection limit of elements ranged from 1μg/L (Co, Mn and Mg) to 55μg/L (Pb). The optimal sample uptake rate and the optimal flow rate of Ar into the nebulizer were found to be 1.33 m1/min and 0.351/min, respectively The optimum nitric acid concentration was 1M. Mn (0.7 μg/g) and Cd (1.2 μg/g) in bone samples were present in the lowest concentrations, and Ca (82007.9 μg/g) and Mg (3005.2 μg/g) had the highest concentrations. Except for Cu, there were no significant differences in element concentrations between males and females. There was a high variation in element concentrations among the bone samples. Conclusions. Further research is needed to investigate the factors that influence the concentrations of elements in bone. The optimal conditions for bone-element analysis using ICPAES as recommended by the authors was confirmed in this study." @default.
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- W2281881434 date "2001-09-01" @default.
- W2281881434 modified "2023-09-27" @default.
- W2281881434 title "Determination of Fourteen Elements in Bone Samples Using Inductively Coupled Plasma (ICP) Analysis" @default.
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- W2281881434 doi "https://doi.org/10.6558/mtjm.2001.6(3).1" @default.
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