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- W2283419688 abstract "Abstract Phase morphology is an important factor in the determination of properties of polymer blends. In this work, methods for determining phase morphology of unvulcanized natural rubber (NR)/high-density polyethylene (HDPE) blends were investigated. Small, quick-quenched samples were taken from the internal mixer for examination under scanning electron microscopy (SEM). There was almost no interruption of the mixing because the sampling device was designed for preventing the coalescence of dispersed particles. Three specimen-preparation methods for SEM were considered: (i) OsO4 vapor staining, followed by carbon coating; (ii) toluene etching of NR phase at room temperature, followed by coating of the surface with a platinum alloy; (iii) crosslinking of NR phase by S2Cl2 vapor and then etching of HDPE phase by using boiling xylene. Method (i), OsO4 staining of cryogenic microtomed samples, was selected for the work on the kinetics of dispersion during the mixing process. Vast differences in phase morphology were observed among the types of samples: quick quenched, cold pressed, and compression molded. We considered the quick-quenched samples to have the phase morphology, which was the most similar to that of the blend during its mixing." @default.
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- W2283419688 date "1998-11-01" @default.
- W2283419688 modified "2023-09-24" @default.
- W2283419688 title "The Evolution of Morphology in NR/HDPE Blends. Part I. Microscopy for Unvulcanized Blends" @default.
- W2283419688 doi "https://doi.org/10.5254/1.3538522" @default.
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