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- W2284101970 abstract "Ex situ analyses of substances extracted from flames provide useful albeit mostly qualitative information on the formation process of soot and on the impact of exhausts on the environment. An experimental setup based on the coupling of laser desorption, laser ionization and time-of-flight mass spectrometry (LD/LI/ToF-MS) is presented in past works as an alternative means to more traditional techniques like gas chromatography (GC) to characterize the polycyclic aromatic hydrocarbons (PAHs) content of soot. In this paper, we go one step further in the understanding of the laser desorption/laser ionization dynamics and propose a combined experimental/simulation approach: we estimate the limit of detection of LD/LI/ToF-MS as low as [0.2, 2.8] fmol per laser pulse and we make quantitative predictions on the concentration of PAHs desorbed from soot. In particular, external calibration with model samples where PAHs are adsorbed on black carbon at known concentrations allows us to link the concentration of PAHs desorbed and detected by photoionization ToF-MS to the concentration of PAHs adsorbed on soot. The comparison of data obtained from the analysis of flame sampled soot with standard commercial GC–MS run in parallel validates the approach and defines limits and potentialities of both techniques." @default.
- W2284101970 created "2016-06-24" @default.
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- W2284101970 date "2015-08-12" @default.
- W2284101970 modified "2023-10-14" @default.
- W2284101970 title "Progress toward the Quantitative Analysis of PAHs Adsorbed on Soot by Laser Desorption/Laser Ionization/Time-of-Flight Mass Spectrometry" @default.
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- W2284101970 doi "https://doi.org/10.1021/acs.est.5b02703" @default.
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