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• W2284365929 endingPage "1818" @default.
• W2284365929 startingPage "1810" @default.
• W2284365929 abstract "We used a high-pressure differential scanning calorimeter (HP-DSC) to study polymer plasticization by compressed gases at pressures of up to 30 MPa for polylactide (PLA), polycarbonate (PC), isotactic polypropylene (iPP), and polystyrene (PS). The pressure reached values twice as high as the previously published data. We found that the polymer/carbon dioxide (CO2) system’s heating curves have an unidentified endothermic peak above 5 MPa, which turns out to be from CO2’s phase transition. The HP-DSC could accurately determine the depression of the glass transition temperature (Tg), crystallization temperature (Tc), and melting temperature (Tm) of various polymers at low pressures by simply starting at a higher temperature to avoid CO2’s phase transition; however, the increased plasticization effect of the dissolved CO2 lowered the Tg to the level of overlapping with CO2’s phase transition phenomena at elevated pressures, and therefore, the depressed Tg could not be measured above 6 MPa for PLA, PC, or PS. On the other hand, the Tc of iPP decreased with an increase in pressure, whereas Tm values of PLA and iPP decreased slightly with an increase in pressure and then remained almost unchanged above a certain pressure, which may indicate an increased hydrostatic pressure effect at elevated pressures." @default.
• W2284365929 created "2016-06-24" @default.
• W2284365929 creator A5011007277 @default.
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• W2284365929 date "2016-02-23" @default.
• W2284365929 modified "2023-10-16" @default.
• W2284365929 title "Effect of Unexpected CO₂’s Phase Transition on the High-Pressure Differential Scanning Calorimetry Performance of Various Polymers" @default.
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• W2284365929 doi "https://doi.org/10.1021/acssuschemeng.6b00008" @default.
• W2284365929 hasPublicationYear "2016" @default.
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