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- W2286740282 abstract "Abstract The imidazolium salts [(N-alkyl-imidazolyl) methyl] benzotriazole hexafluorophosphate ( L1H : alkyl = n-C4H9, L2H : alkyl = picoly, L3H : alkyl = 9-anthrylmethyl, L4H : alkyl = 1-naphthylmethyl) have been prepared. Mononuclear N-Heterocyclic carbene silver complexes: L1AgPF6 ( 1 ), L2AgPF6 ( 2 ), L3AgPF6 ( 3 ) were synthesized in DMSO. Transmetalation reactions afford the synthesis of the nickel(II) complex L2Ni(PF6)2 ( 4 ). Furthermore, L2H , L3H and L4H were treated with silver oxide in CH3CN to afford other complexes ( 5 , 6 and 7 ). The complexes 5 and 6 formed 1D and 2D supramolecular chains by Ag N bond and intermolecular π-π interactions, respectively, which were found that the carbene carbon atoms of NHCs are not coordinated to silver atom. However, in Complex 7 , silver atoms selectly bind to nitrogen atoms of benzotriazoles and carbon atoms of imidazoles, which afford the dinuclear Ag metallamacrocycles. Complexes 1 – 7 were characterized by single crystal X-ray diffraction, NMR spectroscopy, elemental analysis and powder X-ray diffraction. The catalytic activity of NHC Ni complex 4 for Suzuki−Miyaura cross-coupling was studied." @default.
- W2286740282 created "2016-06-24" @default.
- W2286740282 creator A5006716236 @default.
- W2286740282 creator A5014700860 @default.
- W2286740282 creator A5058985073 @default.
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- W2286740282 creator A5078124585 @default.
- W2286740282 creator A5081430902 @default.
- W2286740282 creator A5090875147 @default.
- W2286740282 date "2016-04-01" @default.
- W2286740282 modified "2023-10-16" @default.
- W2286740282 title "Verstile silver(I) and nickel(II) NHC complexes bearing benzotriazole-function: Synthesis, fluorescence and catalytic property" @default.
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