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- W2287288805 abstract "A new combined approach of crystallization in drying is recently evolving due to the need to stabilize powders produced from biological extracts. The operating conditions play a critical role here in this combined process of solid-phase crystallization and drying because the temperature and moisture content of the particles influence the rate of crystallization. The effects of operating conditions on the rate of drying and degree of crystallinity of lactose have been studied in a pilot-scale spray dryer. Temperature, moisture content, feed flow rate, atomizing air-flow rate, main air-flow rate and particle size have been varied to estimate the range of crystallinity of lactose obtainable in a pilot-scale spray dryer. Modulated Differential Scanning Calorimetry (MDSC) and sorption tests (Water-Induced Crystallization) have been used to assess the degree of crystallinity for freshly spray-dried samples. The range of crystallinity obtained for lactose by varying the operating conditions was from 18% - 72%. Use of a lower inlet temperature increased the crystallinity of the product by 35%. Statistical analysis with t-tests confirmed these differences to be significant with 95% confidence. The results suggest differences between small and pilot-scale spray dryers due to differences in particle sizes and drying rates." @default.
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- W2287288805 date "2010-01-01" @default.
- W2287288805 modified "2023-09-26" @default.
- W2287288805 title "The Effects of Operating Conditions on Lactose Crystallization in a Pilot-scale Spray Dryer" @default.
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