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- W2287583165 abstract "Bu calismada, poli(N-vinil kaprolaktam) mikrojellerinin sentezi ve karakterizasyonu gerceklestirilmistir. Mikrojellerin sentezi, sulu ortamda serbest radikal katilma polimerizasyonu ile emulsiyon polimerizasyonu teknigine gore yapilmistir. Farkli turde baslatici kullaniminin ve farkli reaksiyon sicakliklarinin etkisini belirleyebilmek amaciyla dort farkli mikrojel sentezlenmistir. Mikrojellerin sentezinde baslatici olarak; 2,2’-azobisbutironitril (AIBN) ve 2,2’-azobis(2-metilpropionamid) dihidroklorur (AMPA) kullanilmistir. Mikrojeller, AIBN veya AMPA baslaticilari varliginda 70oC ve 80oC olmak uzere iki farkli sicaklikta sentezlenmistir. Takiben sentezlenen tum mikrojellerin reaksiyon verimleri belirlenmistir. Elde edilen polimerlerin yapisal analizi, Fourier Transform Infrared Spektroskopisi (FTIR) ve Taramali Elektron Mikroskobu (SEM) kullanilarak gerceklestirilmistir. Ayrica tum mikrojel urunlerin, zeta potansiyeli ve partikul boyutu dagilimi olcumleri yapilmistir. Calismada elde edilen sonuclara gore, sentez reaksiyonlari, AMPA baslaticisi varliginda ve 70oC sicakliginda gerceklestirildiginde en yuksek reaksiyon verimi elde edilmistir" @default.
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- W2287583165 date "2014-01-10" @default.
- W2287583165 modified "2023-09-30" @default.
- W2287583165 title "Optimization of Synthesis Conditions of Poly(N-Vinylcaprolactam) Microgels" @default.
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- W2287583165 doi "https://doi.org/10.5578/fmbd.6637" @default.
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