FRINK Linked Data Fragments server

Matches in SemOpenAlex for { <https://semopenalex.org/work/W2287647789> ?p ?o ?g. }

• W2287647789 endingPage "2612" @default.
• W2287647789 startingPage "2600" @default.
• W2287647789 abstract "Following the recent prohibition on the use of BPA for the production of polycarbonate (PC) baby bottles in the European Union, baby bottles made of alternative materials, such as polypropylene, polyethersulphone, polyamide, Tritan™ or silicone, have appeared in the market. An initial study done in previous work applying a liquid-liquid extraction (LLE) followed by GC-MS analysis identified a wide variety of migrating compounds. Based on these screening results, the monitoring and quantification of the most important migrating compounds was further pursued. We describe the optimisation, validation and application of an LLE method for the extraction of these migrating compounds adapted to low concentrations. Generally, absolute recoveries between 70 and 110 % with RSDs < 20 % were obtained. Further, specific and quantitative GC-QqQ-MS and LC-QqQ-MS methods were developed and validated by evaluating the following parameters: sensitivity, selectivity, linearity, accuracy, precision, recoveries and matrix effects. Limits of quantification (LOQs) ranged between 0.6 and 8 μg kg−1 for the majority of the selected compounds. Linearity ranged using Mandel’s fitting test between coefficients of determination (R 2) of 0.995 and 0.999. Both repeatability and reproducibility were demonstrated to be satisfactory considering the Horwitz equation. Finally, the methods were applied on a selection of baby bottles representative for the Belgian market. Several compounds previously identified by the screening approach were confirmed and adequately quantified. For instance, azacyclotridecan-2-one had a maximum migration value of 1091 μg kg−1 whereas 4-propylbenzaldehyde migrated at 27 μg kg−1 and 2,2,4-trimethyl-1,3-pentanediol diisobutyrate (TXIB) at 348 μg kg−1. However, most of the targeted compounds were not detected or below the LOQ." @default.
• W2287647789 created "2016-06-24" @default.
• W2287647789 creator A5005602789 @default.
• W2287647789 creator A5014995002 @default.
• W2287647789 creator A5038085199 @default.
• W2287647789 creator A5042123511 @default.
• W2287647789 creator A5051601487 @default.
• W2287647789 creator A5067430326 @default.
• W2287647789 date "2016-02-23" @default.
• W2287647789 modified "2023-10-18" @default.
• W2287647789 title "Quantitative Determination of Migrating compounds from Plastic Baby Bottles by Validated GC-QqQ-MS and LC-QqQ-MS Methods" @default.
• W2287647789 cites W104740688 @default.
• W2287647789 cites W1496723448 @default.
• W2287647789 cites W1971194701 @default.
• W2287647789 cites W1987836585 @default.
• W2287647789 cites W1999482197 @default.
• W2287647789 cites W2007330469 @default.
• W2287647789 cites W2017960722 @default.
• W2287647789 cites W2025094207 @default.
• W2287647789 cites W2027487251 @default.
• W2287647789 cites W2032308113 @default.
• W2287647789 cites W2039562024 @default.
• W2287647789 cites W2044358813 @default.
• W2287647789 cites W2057299122 @default.
• W2287647789 cites W2062772543 @default.
• W2287647789 cites W2083531492 @default.
• W2287647789 cites W2086728307 @default.
• W2287647789 cites W2091957971 @default.
• W2287647789 cites W2093018800 @default.
• W2287647789 cites W2097327668 @default.
• W2287647789 cites W2109847439 @default.
• W2287647789 cites W2113268751 @default.
• W2287647789 cites W2119347390 @default.
• W2287647789 cites W2124807872 @default.
• W2287647789 cites W2137020461 @default.
• W2287647789 cites W2140321480 @default.
• W2287647789 cites W2151572760 @default.
• W2287647789 cites W2241828927 @default.
• W2287647789 cites W2280765446 @default.
• W2287647789 cites W2280840461 @default.
• W2287647789 cites W2519052823 @default.
• W2287647789 cites W2911690791 @default.
• W2287647789 cites W816285861 @default.
• W2287647789 doi "https://doi.org/10.1007/s12161-016-0451-4" @default.
• W2287647789 hasPublicationYear "2016" @default.
• W2287647789 type Work @default.
• W2287647789 sameAs 2287647789 @default.
• W2287647789 citedByCount "12" @default.
• W2287647789 countsByYear W22876477892016 @default.
• W2287647789 countsByYear W22876477892017 @default.
• W2287647789 countsByYear W22876477892018 @default.
• W2287647789 countsByYear W22876477892019 @default.
• W2287647789 countsByYear W22876477892020 @default.
• W2287647789 countsByYear W22876477892021 @default.
• W2287647789 countsByYear W22876477892022 @default.
• W2287647789 countsByYear W22876477892023 @default.
• W2287647789 crossrefType "journal-article" @default.
• W2287647789 hasAuthorship W2287647789A5005602789 @default.
• W2287647789 hasAuthorship W2287647789A5014995002 @default.
• W2287647789 hasAuthorship W2287647789A5038085199 @default.
• W2287647789 hasAuthorship W2287647789A5042123511 @default.
• W2287647789 hasAuthorship W2287647789A5051601487 @default.
• W2287647789 hasAuthorship W2287647789A5067430326 @default.
• W2287647789 hasBestOaLocation W22876477892 @default.
• W2287647789 hasConcept C105639569 @default.
• W2287647789 hasConcept C119128265 @default.
• W2287647789 hasConcept C144133560 @default.
• W2287647789 hasConcept C154020017 @default.
• W2287647789 hasConcept C162356407 @default.
• W2287647789 hasConcept C178790620 @default.
• W2287647789 hasConcept C185592680 @default.
• W2287647789 hasConcept C205345274 @default.
• W2287647789 hasConcept C2777973245 @default.
• W2287647789 hasConcept C2910001868 @default.
• W2287647789 hasConcept C43617362 @default.
• W2287647789 hasConcept C4725764 @default.
• W2287647789 hasConcept C9893847 @default.
• W2287647789 hasConceptScore W2287647789C105639569 @default.
• W2287647789 hasConceptScore W2287647789C119128265 @default.
• W2287647789 hasConceptScore W2287647789C144133560 @default.
• W2287647789 hasConceptScore W2287647789C154020017 @default.
• W2287647789 hasConceptScore W2287647789C162356407 @default.
• W2287647789 hasConceptScore W2287647789C178790620 @default.
• W2287647789 hasConceptScore W2287647789C185592680 @default.
• W2287647789 hasConceptScore W2287647789C205345274 @default.
• W2287647789 hasConceptScore W2287647789C2777973245 @default.
• W2287647789 hasConceptScore W2287647789C2910001868 @default.
• W2287647789 hasConceptScore W2287647789C43617362 @default.
• W2287647789 hasConceptScore W2287647789C4725764 @default.
• W2287647789 hasConceptScore W2287647789C9893847 @default.
• W2287647789 hasFunder F4320324595 @default.
• W2287647789 hasIssue "9" @default.
• W2287647789 hasLocation W22876477891 @default.
• W2287647789 hasLocation W22876477892 @default.
• W2287647789 hasOpenAccess W2287647789 @default.
• W2287647789 hasPrimaryLocation W22876477891 @default.
• W2287647789 hasRelatedWork W1966679081 @default.
• W2287647789 hasRelatedWork W1980714464 @default.

• next