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- W2291130127 abstract "A novel platinum complex with 1,3-bis(2,6-diisopropylphenyl)-1,3-dihydro-2H-imidazol-2-ylidenyl ligand has been synthesized and characterized on the basis of elemental analysis, MS, 1H and 13C NMR spectroscopy, X-ray Absorption Spectroscopy and single crystal X-ray diffraction studies. The XRD determination of the complex (monoclinic, C2/c) revealed a structure in which the platinum (II) centre coordinates two chlorides, a carbon atom of the N-heterocyclic carbene (NHC) and is stabilized by coordinating the nitrogen atom of a 3-chloropyridine molecule, forming an over-all square planar geometry. By prolonging the time of the reaction, it was possible to obtain the trans-dichloridobis(3-chloropyridine) platinum(II) complex under the same reaction conditions. The electronic and molecular properties of both complexes were investigated and compared by means of Near Edge X-ray Absorption Fine Structure spectroscopy (NEXAFS), supported by numerical simulations. The platinum carbene complex obtained was tested in a series of C–H activation and hydrosilylation reactions." @default.
- W2291130127 created "2016-06-24" @default.
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- W2291130127 date "2016-04-01" @default.
- W2291130127 modified "2023-10-04" @default.
- W2291130127 title "Synthesis, spectroscopic characterization and catalytic activity of platinum(II) carbene complexes" @default.
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- W2291130127 doi "https://doi.org/10.1016/j.ica.2016.02.036" @default.
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