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• W2293115780 abstract "The low-temperature fluorination of the n = 2 Ruddlesden-Popper phase La2SrCr2O7 yields La2SrCr2O7F2 via a topochemical fluorine insertion reaction. The structure-conserving nature of the fluorination reaction means that the chromium centers of the initial oxide phase retain an octahedral coordination environment in the fluorinated product, resulting in a material containing an extended array of apex-linked Cr(4+)O6 units. Typically materials containing networks of octahedrally coordinated Cr(4+) centers can only be prepared at high pressure; thus, the preparation of La2SrCr2O7F2 demonstrates that low-temperature topochemical reactions offer an alternative synthesis route to materials of this type. Neutron diffraction, magnetization, and μ(+)SR data indicate that La2SrCr2O7F2 undergoes a transition to an antiferromagnetic state below TN ≈ 140 K. The structure-property relations of this phase and other Cr(4+) oxide phases are discussed." @default.
• W2293115780 created "2016-06-24" @default.
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• W2293115780 date "2016-03-09" @default.
• W2293115780 modified "2023-09-23" @default.
• W2293115780 title "La₂SrCr₂O₇F₂: A Ruddlesden–Popper Oxyfluoride Containing Octahedrally Coordinated Cr⁴⁺ Centers" @default.
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• W2293115780 doi "https://doi.org/10.1021/acs.inorgchem.6b00114" @default.
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