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- W2293801117 abstract "One of the major challenges in structural characterization of oligosaccharides is the presence of many structural isomers in most naturally occurring glycan mixtures. Although ion mobility spectrometry (IMS) has shown great promise in glycan isomer separation, conventional IMS separation occurs on the millisecond time scale, largely restricting its implementation to fast time-of-flight (TOF) analyzers which often lack the capability to perform electron activated dissociation (ExD) tandem MS analysis and the resolving power needed to resolve isobaric fragments. The recent development of trapped ion mobility spectrometry (TIMS) provides a promising new tool that offers high mobility resolution and compatibility with high-performance Fourier transform ion cyclotron resonance (FTICR) mass spectrometers when operated under the selected accumulation-TIMS (SA-TIMS) mode. Here, we present our initial results on the application of SA-TIMS-ExD-FTICR MS to the separation and identification of glycan linkage isomers." @default.
- W2293801117 created "2016-06-24" @default.
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- W2293801117 date "2016-03-14" @default.
- W2293801117 modified "2023-10-15" @default.
- W2293801117 title "Separation and Identification of Isomeric Glycans by Selected Accumulation-Trapped Ion Mobility Spectrometry-Electron Activated Dissociation Tandem Mass Spectrometry" @default.
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- W2293801117 doi "https://doi.org/10.1021/acs.analchem.6b00041" @default.
- W2293801117 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/4821751" @default.
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