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• W2296209557 abstract "A simple and convenient procedure for the synthesis of some novel alkyl‐substituted and aryl‐substituted julolidines is reported. Julolidines were smoothly synthesized in excellent isolated yields via Friedel–Crafts intramolecular alkylations of heteroarylalkanols in the presence of both Brønsted (PPA) and Lewis (AlCl 3 /CH 3 NO 2 ) acid catalysts. The precursors alkanols, 1a , 1b , 1c , 1d , 1e , 1f , 1g , 1h , 1i , were readily prepared both by reaction of selectively synthesized carboxylic acid esters and ketones with different Grignard reagents and also by reduction of the synthesized ketones with LAH. A plausible carbocation mechanism is proposed to account for the results. The structures of the compounds are established using both spectral and analytical data." @default.
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• W2296209557 date "2013-10-31" @default.
• W2296209557 modified "2023-10-04" @default.
• W2296209557 title "Modern Friedel-Crafts Chemistry. Part 37. Efficient Syntheses of Some New Julolidines via Cyclialkylations of Heteroaryl Carbinols" @default.
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• W2296209557 doi "https://doi.org/10.1002/jhet.1797" @default.
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