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- W2297666585 abstract "Many inorganic compounds show significant deviations from stoichiometric composition; this is true of the oxides of uranium. The preparation of stoichiometric U/sub 3/C/sub 8/ depends on the starting uranium compound, sample size (bed depth), temperature, duration of ignition, and any chemical alteration of the starting compound. Stoichiometric U/sub 3/O/sub 8/ was prepared in 10-g quantities from uranyl fluoride and uranium peroxide by ignition at 850 gas- cooled C for 16 hr and from uranyl nitrate and uranium trioxide by ignition at 1000 gas-cooled C for 16 hr followed by reignition at 850 gas-cooled C to constant weight. Long periods of ignition to form the stoichiometric oxide are not required in the specialized gravimetric method presented for the determination of uranium. (auth)" @default.
- W2297666585 created "2016-06-24" @default.
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- W2297666585 date "1960-11-30" @default.
- W2297666585 modified "2023-09-24" @default.
- W2297666585 title "PREPARATION OF STOICHIOMETRIC U$sub 3$O$sub 8$" @default.
- W2297666585 doi "https://doi.org/10.2172/4114102" @default.
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