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- W2299693359 abstract "A series of novel N ‐{5‐[2‐(4,6‐dimethoxy‐pyrimidin‐2‐yloxy)‐phenyl]‐[1,3,4]thiadiazol‐2‐yl}2‐aroxy‐propanamides were designed and synthesized by the multistep reactions. 2‐(4,6‐Dimethoxy‐pyrimidin‐2‐yloxy)‐benzaldehyde ( 1 ) reacted with aminothiourea to yield 2 , which undergoes ring closure to give 5‐[2‐(4,6‐dimethoxy‐pyrimidin‐2‐yloxy)‐phenyl]‐[1,3,4]thiadiazol‐2‐amine ( 3 ) in the presence of ferric chloride in refluxing ethanol. 3 reacted with 2‐aroxy‐propionyl chlorides to give the target compounds 4a , 4b , 4c , 4d , 4e , 4f , 4g , 4h , 4i in moderate to good yields. Their structures were confirmed by IR, 1 H‐NMR, EIMS, and elemental analyses. The preliminary bioassay indicated that some of them displayed moderate to good selective herbicidal activity against Brassica campestris L . at the concentration of 100 mg/L. However, these compounds did not possess inhibitory activity against Echinochloa crus‐galli at the tested concentrations." @default.
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- W2299693359 date "2013-11-18" @default.
- W2299693359 modified "2023-10-04" @default.
- W2299693359 title "Synthesis and Herbicidal Activity of 2-Aroxy-propanamides Containing Pyrimidine and 1,3,4-Thiadiazole Rings" @default.
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- W2299693359 doi "https://doi.org/10.1002/jhet.1853" @default.
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