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- W2300851004 abstract "A novel aromatic diamine-based benzoxazine (P-mPDA) is successfully synthesized from m-phenylenediamine (m-PDA), 2-hydroxybenzaldehyde, and formaldehyde. The polymerization behavior of P-mPDA and the properties of its thermoset are studied. The results indicate that P-mPDA owns favorable processability including low polymerization temperature, low liquefying temperature, and wide processing window. Even lower polymerization temperature (polymerization onset temperature as low as 80 °C) can be achieved by the promotion of catalysts. The ring-opening polymerization of P-mPDA first generates polybenzoxazine with N, O-acetal-type structure and arylamine Mannich-type structure, following which rearrangement from N, O-acetal-type structure to phenolic Mannich-type structure proceeds at elevated temperature. Furthermore, the polymerized P-mPDA shows outstanding performance such as extremely high glass transition temperature (Tg) of 280 °C, high char yield above 53% at 800 °C under nitrogen and excellent mechanical property. © 2016 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2016, 133, 43368." @default.
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- W2300851004 date "2016-01-28" @default.
- W2300851004 modified "2023-09-24" @default.
- W2300851004 title "An<i>m</i>-phenylenediamine-based benzoxazine with favorable processability and its high-performance thermoset" @default.
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- W2300851004 doi "https://doi.org/10.1002/app.43368" @default.
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