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- W2300960100 abstract "We report a simple and sustainable protocol for the synthesis of monodisperse rhodium (Rh), ruthenium (Ru), and palladium (Pd) metal nanoparticles supported on fibrous nanosilica (KCC-1). In this protocol, use of expensive dendrimers was replaced by inexpensive polyethylenimine (PEI) to produce highly monodispersed supported metal nanocatalysts. First, KCC-1 was covalently functionalized by PEI and then metal(II) salts were loaded on KCC-1-PEI material to have complexation of metal ions with amines of PEI. Reduction of metal(II) ions by NaBH4 yielded metal(0) nanoparticles supported on KCC-1. As-synthesized metal nanoparticles supported on PEI functionalized KCC-1, named KCC-1-PEI/Rh, KCC-1-PEI/Ru, and KCC-1-PEI/Pd, were characterized by transmission electron microscopy (TEM) for particle size and their distribution, N2 sorption studies for surface area, pore sizes and pore volume, thermogravimetric analysis for PEI loading, and solid state NMR for its covalent attachment. These nanocatalysts were then ev..." @default.
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- W2300960100 date "2015-10-27" @default.
- W2300960100 modified "2023-10-02" @default.
- W2300960100 title "Efficient Synthesis of Monodisperse Metal (Rh, Ru, Pd) Nanoparticles Supported on Fibrous Nanosilica (KCC-1) for Catalysis" @default.
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- W2300960100 doi "https://doi.org/10.1021/acssuschemeng.5b00812" @default.
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