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- W2303764200 abstract "Total synthesis of the hexasaccharide repeating unit of the O-antigen from Shigella flexneri serotype 1d (I: 7,8), α-D-Glcp-(1→3)-α-L-Rhap-(1→2)-α-L-Rhap-(1→3)-α-L-Rhap-(1→3)-[α-D-Glcp-(1→4)]-β-D-GlcpNAc, is reported by following a linear strategy. The target hexasaccharide was synthesized by sequential glycosylations of suitably protected monosaccharide derivatives prepared from commercially available monosaccharides through rational protecting group manipulations. Stereoselective glycosylations were accomplished by the activation of thioglycoside using N-iodosuccinimide and H2SO4-silica. The use of H2SO4-silica in place of traditional promoters like TfOH or TMSOTf was proved to be a better option for the NIS-mediated thioglycoside activation." @default.
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- W2303764200 date "2016-05-01" @default.
- W2303764200 modified "2023-09-28" @default.
- W2303764200 title "Linear synthesis of the hexasaccharide related to the repeating unit of the O-antigen from Shigella flexneri serotype 1d (I: 7,8)" @default.
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- W2303764200 doi "https://doi.org/10.1016/j.carres.2016.03.012" @default.
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