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- W2304876159 abstract "Purely siliceous MCM-4 1 (SiMCM-4 1) and aluminium-containing MCM-4 1(AIMCM-41) with different ratios of AVSi were synthesized following a modifiedprocedure of Ryoo and Kim (1 995). PolypyrroleJMCM-4 1 (PPyJMCM-4 1)conductive polymer nanocomposite films was electrochemically prepared on IndiumTin Oxide (ITO) glass electrode from an aqueous solution of pyrrole monomer and ptoluenesulfonate dopant in a suspension of prepared MCM-41. Various PPy/MCM-41 nanocomposite films were obtained by varying the experimental conditions withthe objective of producing conductive polymer nanocomposites with enhancedthermal and conductivity properties. The prepared nanocomposite films werecharacterized by Fourier Transform Infrared (FTIR) Spectroscopy, X-ray diffraction(XRD) analysis, Thermogravimetric Analysis, Scanning Electron Microscopy (SEM),Transmission Electron Microscopy (TEM) and conductivity measurements. From observations of the XRD patterns, nanocomposites prepared at low AVSi ratio(PPyJA130 and PPyJA140) and PPyJSiMCM-41 showed better crystallinity comparedto those prepared at high AlJSi ratio (PPyJA160 and PPyJA180) which was observed tobe amorphous. FTIR and XRD studies showed that the PPy and SiMCM-41 are themost compatible for the formation of PPyJSiMCM-41 nanocomposite. The TGAanalysis and conductivity studies showed that the best nanocomposite wasPPyJSiMCM-41 which was found to be the most thermally stable with the highestconductivity of 5.24 SJcm. This sample was obtained with optimum condition with0.5 M pyrrole, 0.1 M p-toluene sulfonate and 3 g/dm3 MCM-41 at 1.2 volt (vs SCE)." @default.
- W2304876159 created "2016-06-24" @default.
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- W2304876159 date "2006-04-01" @default.
- W2304876159 modified "2023-09-24" @default.
- W2304876159 title "Fabrication of Polypyrrole-Mcm41 Nanocomposites Using Electrodeposition Method" @default.
- W2304876159 hasPublicationYear "2006" @default.
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