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• W2307786214 abstract "The title Cu(II) complex, [Cu2(NCS)4(C6H10N4)2], represents the first crystal structure of a polynuclear transition metal complex with the 3,5-dimethyl-1H-pyrazole-1-carboxamidine ligand (HL). It is compared with previously reported crystal structures of metal complexes with the same HL ligand. The molecule contains an eight-membered binuclear Cu2(NCS)2 ring, which is centrosymmetric and in a chair conformation. The Cu atom has a distorted square-pyramidal geometry with a very elongated Cu-S bond of 2.993 (2) A. The crystal structure redetermination of the bis(3,5-dimethyl-1H-pyrazole-1-carboxamidine-kappa(2)N,N')bis(nitrato-kappaO)copper(II)complex, [Cu(NO3)2(C6H10N4)2], and analysis of its hydrogen bonds confirm the significance of the NO3 groups in the formation of a three-dimensional hydrogen-bonding network. Both complexes are centrosymmetric, the inversion centre being located at the mid-point of the Cu...Cu line in (I) and the Cu atom being located at the inversion centre in (II)." @default.
• W2307786214 created "2016-06-24" @default.
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• W2307786214 date "2005-07-09" @default.
• W2307786214 modified "2023-09-24" @default.
• W2307786214 title "Transition metal complexes with pyrazole-based ligands. XXII. Di-μ-thiocyanato-bis[(3,5-dimethyl-1<i>H</i>-pyrazole-1-carboxamidine-κ²<i>N</i>,<i>N</i>′)(thiocyanato-κ<i>N</i>)copper(II)] and a redetermination of bis(3,5-dimethyl-1<i>H</i>-pyrazole-1-carboxamidine-κ²<i>N</i>,<i>N</i>′)bis(nitrato-κ<i>O</i>)copper(II)" @default.
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• W2307786214 doi "https://doi.org/10.1107/s0108270105018913" @default.
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