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- W2309720855 abstract "Abstract A novel electrocatalyst for methanol oxidation reaction in alkaline medium is elaborately fabricated by a sponge-template method involving an electroless plating of amorphous Ni–P on sponge and the following annealing process at 500 °C in air. The electrocatalyst is characterized by NiO nanoparticle/nanoflake grown on the Ni–P alloy tube. The vital annealing process aims to remove templates, crystallize Ni–P, and generate NiO nanostructures on the outside surface of Ni–P tubes, thus leading to the final structure of NiO/Ni–P composites. The tubular Ni–P framework surface is decorated with microspherical NiO (EP-M) or nanoflake NiO (EP-F), which strongly depends on the electroless plating time. For comparison, porous NiO nanoflakes are also synthesized by chemical bath deposition. The EP-M containing ∼83.8 wt.% NiO and ∼16.2 wt.% Ni–P has the largest BET surface area of 210.03 m 2 g −1 among the three samples. Moreover, the EP-M exhibits a high current density (∼467 A g −1 ) and long-term chronoamperometry stability (≥20,000 s) toward methanol oxidation in alkaline solution. The improved catalytic activity of the composite catalyst might be attributed to the strong electronic interaction between NiO and Ni–P as revealed by X-ray photoelectron spectroscopy." @default.
- W2309720855 created "2016-06-24" @default.
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- W2309720855 date "2016-04-01" @default.
- W2309720855 modified "2023-10-17" @default.
- W2309720855 title "Thermal growth of NiO on interconnected Ni–P tube network for electrochemical oxidation of methanol in alkaline medium" @default.
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- W2309720855 doi "https://doi.org/10.1016/j.ijhydene.2016.03.018" @default.
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