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- W2309747155 abstract "Abstract Vasarene is a vase-shaped compound readily obtained by the reaction between ninhydrin and phloroglucinol (1,3,5-benzenetriol). Vasarene has shown a special affinity towards alkali fluoride ion-pairs, forming with them cage-like supramolecular structures composed of several vasarene units encapsulating the alkali fluoride salt. Here we report the preparation and characterization of a series of geometrically modified vasarenes containing only two ‘side-walls’ instead of three, and their derivatives. Synthesis under microwave conditions could be accomplished within minutes compared to hours for ‘regular’ solvent heating. Like vasarene, the new analogues have also demonstrated a selective affinity to alkali- and tetraalkyl ammonium-fluorides including inter alia their solubilization in organic solvents and precipitation from aqueous solutions." @default.
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- W2309747155 date "2016-05-01" @default.
- W2309747155 modified "2023-10-16" @default.
- W2309747155 title "Vasarene and vasarene-analogues: synthesis and characterization of self-assembled, voluminous ligands with specific affinity to M+F− ion-pairs" @default.
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- W2309747155 doi "https://doi.org/10.1016/j.tet.2016.03.065" @default.
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