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- W230981435 abstract "The ethoxymethylation of methylenecyclobutane with epoxymethyl fluorosulfonate, generated in situ from fluoromethyl ethyl ether and sulfur trioxide, with methanol as external nucleophile leads to 1-methoxy-1-(2-ethoxyethyl)cyclobutane. 1-Hydroxy-1-(2-ethoxyethyl)cyclobutane is mainly formed during treatment with a solution of sodium bicarbonate in water, and (2-ethoxyethylidene)cyclobutane and 1-(2-ethoxyethyl)-1-cyclobutene are also formed. Treatment of the reaction mixture with triethylamine leads to (2-ethoxyethylidene)cyclobutane and 1-(2-ethoxyethyl)-1-cyclobutene. The /sup 1/H NMR spectra were recorded on a Tesla BS-467 spectrometer at 60 MHz. The /sup 13/C NMR spectra were obtained on a Varian FT-80 instrument at 20 MHz in carbon tetrachloride." @default.
- W230981435 created "2016-06-24" @default.
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- W230981435 date "1987-10-10" @default.
- W230981435 modified "2023-09-23" @default.
- W230981435 title "Ethoxymethyl fluorosulfonate. Stage-by-stage addition of ethoxymethyl group and external nucleophile to methylenecyclobutane" @default.
- W230981435 hasPublicationYear "1987" @default.
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