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- W2312413252 abstract "The phase diagrams of the systems ABr/SmBr3 were reinvestigated. The findings of Blachnik for the systems withA=Cs, Rb, K were confirmed; however, the dimorphic compound K3SmBr6 is stable only above 572 K. The equilibrium temperature, found bye.m.f.-measurements in a solid state galvanic cell for the reaction KBr+K2SmBr5=L-K3SmBr6, is smaller (522 K). The formation temperature for Rb3SmBr6 is 279 K (DTA) and 256 K (e.m.f.) resp. By solution calorimetry was proved that the compounds Cs2SmBr5 and KSm2Br7 don't exist at 0 K. In the system NaBr/SmBr3 only one hitherto unknown dimorphic compound Na3SmBr3 exists above 473 K. L-Na3SmBr crystallizes in the hexagonal space groupR¯3, above 519 K H-Na3SmBr6 has the monoclinic cryolite-structure. Powder patterns of other compounds not yet investigated — H-/L-A3 SmBr6, ASm2Br7 (A=Cs, Rb, K) and Cs2SmBr5 — were indexed analogously to known structure families. The structure parameters of SmBr3·6H2O were determined by single-crystal measurements." @default.
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- W2312413252 date "1996-05-01" @default.
- W2312413252 modified "2023-09-24" @default.
- W2312413252 title "Thermochemical and structural investigations" @default.
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- W2312413252 doi "https://doi.org/10.1007/bf01979238" @default.
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