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- W2313285441 abstract "The C–Si bonds of triisopropylsilyl-substituted alkenes, 1,3-dienes, and related multifunctional substrates, as well as analogous C–TBDPS and C–TBS bonds, are readily and chemoselectively cleaved with NIS (or other sources of I+, such as N-iodosaccharin, 1,3-diodohydantoin, and Ipy2BF4). The desired iodoalkenes are obtained stereospecifically without byproducts, provided that the reactions are carried out in CF3CHOHCF3 and, in general, with 30 mol % of Ag2CO3 (or AgOAc/2,6-lutidine) as an additive. Fragment C10–C18 of cytotoxic amphidinolides B1–B3 and D has been synthesized using this improved procedure." @default.
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- W2313285441 date "2011-08-25" @default.
- W2313285441 modified "2023-09-30" @default.
- W2313285441 title "Iododesilylation of TIPS-, TBDPS-, and TBS-Substituted Alkenes in Connection with the Synthesis of Amphidinolides B/D" @default.
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- W2313285441 doi "https://doi.org/10.1021/ol2020187" @default.
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