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• W2313372642 abstract "The synthesis of a transition metal nitride, Ta3N5, was studied. Morphological changes of Ta3N5 particles, depending on the synthetic method, starting materials, and nitridation conditions, were examined in detail. Flux-assisted nitridation was found to be a facile one-step route to a metal nitride with morphological control of the resulting particles. Scanning electron microscopy (SEM) observation revealed that morphologically defined particles of Ta3N5 were obtained using Zn, NaCl, or Na2CO3 as a flux. Flux-assisted nitridation of TaCl5 with Zn or NaCl produced nearly monodisperse fine particles larger than a few tens of nanometers. The size of these particles could be controlled by variation of the nitridation temperature. Highly crystallized Ta3N5 particles with a rectangular parallelepiped shape were produced from TaCl5−NaCl or Ta2O5−Na2CO3 mixtures by nitridation above 1123 K, because of the annealing effect of the flux." @default.
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• W2313372642 date "2010-11-23" @default.
• W2313372642 modified "2023-10-03" @default.
• W2313372642 title "Synthesis of Structurally Defined Ta₃N₅ Particles by Flux-Assisted Nitridation" @default.
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• W2313372642 doi "https://doi.org/10.1021/cg901025e" @default.
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