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- W2313448581 abstract "Regioselective alkylation of γ-cyclodextrin with allyl or propargyl bromide, using optimized reaction conditions, followed by peracetylation of the remaining hydroxyl groups and separation of isomers resulted in the set of peracetylated 2(I)-O-, 3(I)-O- and 6(I)-O-alkylated cyclodextrins in up to 19% yields. Ozonolysis or oxidative cleavage of peracetylated allyl derivatives resulted in a complete set of peracetylated 2(I)-O-, 3(I)-O-, and 6(I)-O-formylmethyl or -carboxymethyl derivatives. All of these derivatives are useful precursors for further preparation of regioselectively monosubstituted derivatives of γ-cyclodextrin." @default.
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- W2313448581 date "2012-12-17" @default.
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- W2313448581 title "Complete Sets of Monosubstituted γ-Cyclodextrins as Precursors for Further Synthesis" @default.
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- W2313448581 doi "https://doi.org/10.1021/jo301656p" @default.
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