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• W2313894178 abstract "We present a facile route to prepare selenium nanorods (SeNRs) with alternating symmetry-breaking segments dispersed in aqueous solution. The key roles in this preparation include an assistance provided by the carboxymethyl–cellulose (CMC) and a careful control in particle’s nucleation and growth. Thus, prepared symmetry-breaking segmented SeNRs, namely, SBS-SeNRs, show discrete trigonal and quasi-trigonal phases in the form of repeating quasi-trigonal–trigonal–quasi-trigonal, (tq–t–tq)n, where tq stands for the quasi-trigonal phase in the space group of P321 and t is the trigonal phase in the space group of P3121. Evidence from the particle dimensions analysis during the growth and the result of post-synthesis surface modification showed that the SBS-SeNRs grow via two different particle couplings. The first one was found in the early stage that very short monoclinic Se nanorods couple together with a simultaneous phase transition to trigonal SeNR. The second coupling occurs at the later stage by the coupling of the (tq–t–tq)-SeNRs, which are formed via a growth of symmetry-breaking Se at both ends of the t-SeNR. Meanwhile, we designed an experiment by conducting the silica coating via sol–gel process to further prove the symmetry-breaking segmented nanostructure. The coating proceeded preferentially on the trigonal segments of SBS-SeNRs rather than the quasi-trigonal segments to form a float-like core−shell nanostructure, as well as a string of beads-like one in the case of selenium nanowires (SeNWs). The synthesis of SBS-SeNRs demonstrates the segmented nanomaterials are no longer limited in the combination of different compositions, but opens up a possibility for the versatile intriguing segmented nanomaterials in the future." @default.
• W2313894178 created "2016-06-24" @default.
• W2313894178 creator A5016193741 @default.
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• W2313894178 date "2015-04-08" @default.
• W2313894178 modified "2023-09-28" @default.
• W2313894178 title "Symmetry-Breaking Segmented Selenium Nanorods and Nanowires: Synthesis via Coupling of Nanorods" @default.
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• W2313894178 doi "https://doi.org/10.1021/cm504522y" @default.
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