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• W2313961736 endingPage "14427" @default.
• W2313961736 startingPage "14419" @default.
• W2313961736 abstract "Superconducting (SC) and non-superconducting (non-SC) RbxFe2–ySe2 crystals were grown using the “self-flux” technique in order to assign the microstructural changes to the onset of superconductivity in complex iron selenides. The crystals were thoroughly characterized by magnetic susceptibility and transport measurements as well as powder X-ray diffraction. Special attention was paid to the comparison of the microstructure of the crystals with and without the superconducting transition by means of transmission electron microscopy (TEM). It is shown that the alternation of ordered and disordered regions on the sample surface and along the c-axis is characteristic for both SC and non-SC materials and therefore does not necessarily represent a trigger of superconductivity. Three types of electron diffraction patterns were found for the superconducting RbxFe2–ySe2 sample, of which one is observed for the first time and originates from alkali metal ordering. Moreover, for the superconducting RbxFe2–ySe2 material a monoclinic distortion with β ∼ 87° was observed, leading to the space group I2/m. This monoclinic distortion seems to be an attribute of the superconducting material only, whereas in the non-superconducting sample the orthogonality of the crystallographic axes is preserved." @default.
• W2313961736 created "2016-06-24" @default.
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• W2313961736 date "2013-11-27" @default.
• W2313961736 modified "2023-10-05" @default.
• W2313961736 title "Diversity of Microstructural Phenomena in Superconducting and Non-superconducting Rb_<i>x</i>Fe_2–<i>y</i>Se₂: A Transmission Electron Microscopy Study at the Atomic Scale" @default.
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• W2313961736 doi "https://doi.org/10.1021/ic402710r" @default.
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