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• W2314553675 startingPage "944" @default.
• W2314553675 abstract "Iron-based N-heterocyclic carbene (FeX3(NHC)) complexes were used in initiators for continuous activator regeneration atom transfer radical polymerization (ICAR ATRP). A series of ICAR ATRPs of methyl methacrylate (MMA) and styrene (St) were carried out using FeX3(IDipp) where IDipp = 1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene with X = Cl (I–Cl) or Br (I–Br) and FeX3(HIDipp) (HIDipp =1,3-bis(2,6-diisopropylphenyl)imidazolidin-2-ylidene) with X = Cl (H–Cl) or Br (H–Br). The polymerizations showed good activity, resulting in polymers with controlled molecular weights and narrow molecular weight distribution (MWD) with low loading of catalysts (50 ppm). In particular, I–Br and H–Br generated polymers with narrower MWD. For example, ICAR ATRP of MMA with 50 ppm catalysts (H–Br) after 24 h at T = 60 °C in 50% v/v anisole resulted in PMMA with Mw/Mn = 1.20 at 65% monomer conversion. ICAR ATRP of St after 72 h resulted in PSt with Mw/Mn = 1.15 at 53% monomer conversion." @default.
• W2314553675 created "2016-06-24" @default.
• W2314553675 creator A5056539244 @default.
• W2314553675 creator A5078083709 @default.
• W2314553675 creator A5087023232 @default.
• W2314553675 date "2014-09-04" @default.
• W2314553675 modified "2023-10-17" @default.
• W2314553675 title "Initiators for Continuous Activator Regeneration Atom Transfer Radical Polymerization of Methyl Methacrylate and Styrene with <i>N</i>-Heterocyclic Carbene as Ligands for Fe-Based Catalysts" @default.
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• W2314553675 doi "https://doi.org/10.1021/mz500539j" @default.
• W2314553675 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/35596365" @default.
• W2314553675 hasPublicationYear "2014" @default.
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