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• W2314593602 abstract "Distribution and dynamics of methyl methacrylate (MMA) in contact with polystyrene-block-poly(methacrylic acid) micelles under the conditions of its full solubility in D2O (2 g/L) were studied by 1H NMR methods, in particular pulsed-gradient-stimulated echo (PGSE), transverse relaxation, and rotating-frame relaxation, under varying intensity of the spin-lock field. It was found that MMA can penetrate into the micellar core after many hours at 300 K. In a freshly prepared system, MMA resides almost exclusively in the micellar shell. Its radial distribution there can be described by a Gaussian function with a maximum at the core−shell interface and a mean scatter of about 1.66 × R, where R is the radius of the core. Although it is fairly stable during the rotational and translational diffusion of the micelle as a whole, this distribution has an internal dynamics. According to the combined results of NMR, individual MMA molecules exchange their residence sites with an average correlation time of about 5 × 10-4 s. Transient sorption of MMA molecules to methacrylic acid units is discussed as a probable explanation of this dynamics." @default.
• W2314593602 created "2016-06-24" @default.
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• W2314593602 date "2000-11-10" @default.
• W2314593602 modified "2023-10-16" @default.
• W2314593602 title "Distribution and Dynamics of a Low-Molecular-Weight Solute in the Shell of a Polymer Micelle As Studied by Nuclear Magnetic Resonance" @default.
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• W2314593602 doi "https://doi.org/10.1021/la000832a" @default.
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