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- W2315238909 abstract "Effective and convenient protocols using renewable sugar-derived palladium(0) nanoparticles (PdNPs) as in situ-formed catalysts for Suzuki–Miyaura cross-coupling reactions in isopropanol under thermal and microwave heating conditions have been developed. The addition of a small amount of glucose (5 mol %) to the reaction mixture lead to an increase in yield of the cross-coupled products compared to control experiments that omitted glucose. The size and morphology of the in situ-formed PdNPs were determined by TEM, and further EF-TEM analysis showed a hydrophilic hydroxylated shell around the individual palladium particles. The polar/hydrophilic nature of the nanoparticles allowed for their facile removal from the cross-coupled product, and a significant decrease in the amount of palladium incorporated into the final product was observed, as measured by ICP-MS analysis." @default.
- W2315238909 created "2016-06-24" @default.
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- W2315238909 date "2013-11-21" @default.
- W2315238909 modified "2023-09-26" @default.
- W2315238909 title "Glucose-Derived Palladium(0) Nanoparticles as in Situ-Formed Catalysts for Suzuki–Miyaura Cross-Coupling Reactions in Isopropanol" @default.
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- W2315238909 doi "https://doi.org/10.1021/sc400410v" @default.
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