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• W2315599666 abstract "A thin and well-intergrown zeolite T membrane with high CO2 permeability and selectivity was rapidly prepared on seeded tubular supports by the two-step varying-temperature hydrothermal synthesis process (two-step method). The influence of synthesis parameters such as synthesis temperature and crystallization time during the two-step durations on crystals growth and separation performance was investigated systematically. The X-ray diffraction (XRD), scanning electron microscopy (SEM), and gas permeation measurements were used to characterize the as-synthesized membranes. Compared with the conventional hydrothermal synthesis at a constant temperature (one-step method), the two-step method is more effective to synthesize a thin and continuous zeolite membrane layer in short time, which fully covered the support surface. Membrane synthesis temperature during the two-step durations could seriously influence the crystal growth and CO2 separation properties. It was found that a lower temperature favored nucleation, while a higher crystallization temperature promoted crystallization during the two-step method, thus improving zeolite T crystal growth and membrane separation properties. The membranes prepared by the two-step method under the optimized conditions exhibited good reproducibility, high CO2 permeance, and relatively high permselectivity for the separation of CO2 from CH4 or N2 gas mixtures. For example, CO2 permeance and CO2/CH4 selectivity of the membranes reached 6.2 × 10–8 mol m–2 s–1 Pa–1 and 80 for the equimolar CO2/CH4 binary gaseous mixtures at 35 °C, respectively." @default.
• W2315599666 created "2016-06-24" @default.
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• W2315599666 date "2013-11-06" @default.
• W2315599666 modified "2023-09-28" @default.
• W2315599666 title "Preparation of Zeolite T Membranes by a Two-Step Temperature Process for CO₂ Separation" @default.
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• W2315599666 doi "https://doi.org/10.1021/ie4025402" @default.
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