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- W2315702907 abstract "Three 3D supramolecular networks, [Co(H2L1)2]·(SO4)·2H2O (1), [Co(H2L1)(SO4)(H2O)(DMF)] (2), and [Co(H2L2)(SO4)(H2O)] (3), were prepared by reacting Co(II) sulfate with the rigid bis-imidazoles of 1,4-di(1H-imidazol-4-yl)benzene (H2L1) and 1,3-di(1H-imidazol-4-yl)benzene (H2L2) in solvothermal conditions. Compounds 1 and 2 containing the H2L1 ligand were isolated under different solvent-pair ratios. The structure of 1 can be described as a 6-fold interpenetrating 3D dia net in which the sulfate anions are positioned in the void spaces to balance the overall charge of the framework. In comparison, complex 2 shows a rectangular 2D grid consisting of 1D sulfate-bridged chains linked by H2L1. When H2L2 is used in the reaction, the complex 3 having a 3D interdigitaed network with helical chains is formed, which is the first example of an H2L2-connected coordination polymer. The sulfate ions essentially contribute to the entanglement of the structures through extensive hydrogen bonding. Magnetic measurements for 2 indicate that very weak ferromagnetic interactions are operative between anisotropic Co(II) centers via sulfate bridges." @default.
- W2315702907 created "2016-06-24" @default.
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- W2315702907 date "2012-04-18" @default.
- W2315702907 modified "2023-09-27" @default.
- W2315702907 title "Sulfate-Incorporated Co(II) Coordination Frameworks with Bis-imidazole Bridging Ligands Constructed by Covalent and Noncovalent Interactions" @default.
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- W2315702907 doi "https://doi.org/10.1021/cg300302n" @default.
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