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- W2316149257 abstract "A convergent route to multigram quantities of a mineralocorticoid antagonist 3 is described. Starting from (R)-phenylglycinol, the synthesis of cis 2,5-morpholine 2 is accomplished utilizing a de-epimerization to install the second stereogenic center. The multigram synthesis of 3 was completed through a sequence of an SNAr reaction, Dakin oxidation, alkylation, and cyclization to provide a crystalline solid." @default.
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- W2316149257 date "2013-05-20" @default.
- W2316149257 modified "2023-09-27" @default.
- W2316149257 title "Synthesis of a <i>cis</i> 2,5-Disubstituted Morpholine by De-epimerization: Application to the Multigram Scale Synthesis of a Mineralocorticoid Antagonist" @default.
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- W2316149257 doi "https://doi.org/10.1021/op400101p" @default.
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