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- W2316352852 abstract "A thermal-initiated polymerization procedure is described for the controlled preparation of monodispersed polyacrylamide (PAM) hydrogel microspheres. A coaxial microfluidic device was designed to disperse uniform drops (∼500 μm) of acrylamide monomer aqueous solution into n-octane. Using a delay loop immersed into a heat bath, the polymerization is initiated and carried out in separate droplets. Combining the improvement of heat transfer in the microfluidic device and the sufficient addition of n-octane, the controllable preparation can still be achieved at 95 °C, much higher than 20–60 °C as reported prevalently. Herein, the PAM microspheres can be prepared within 2 min or less, with the CV of diameter less than 4%. Furthermore, based on this controllable reaction platform, PAM microspheres were prepared at various reaction temperatures (higher than 90 °C) and monomer solution compositions to investigate the fundamental rules of controlling on their skeleton structure and absorbent capacity in deionized water." @default.
- W2316352852 created "2016-06-24" @default.
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- W2316352852 date "2012-06-22" @default.
- W2316352852 modified "2023-09-23" @default.
- W2316352852 title "Controllable Preparation of Polyacrylamide Hydrogel Microspheres in a Coaxial Microfluidic Device" @default.
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- W2316352852 doi "https://doi.org/10.1021/ie3004013" @default.
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